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There is a long way for OGSA to go before there is complete architecture speci cation where all of the desired properties of the Grid are addressed. OGSA will have to be re ned and adjusted iteratively, but this is a natural and healthy process, and the rst very important step has been taken. It is felt that this step has been taken in the right direction and we hope that OGSA will be successful in its evolution into the open standards-based architecture that it sets out to de ne. Kunszt [28] points out some issues remain to be resolved in the future development of OGSA with respect to aspects such as availability, robustness, scalability, measurability, interoperability, compatibility, service discovery, manageability and changeability. Dialani et al. [29] propose a transparent fault tolerance mechanism for Web services that may be used to support Grid services fault tolerance. A service may become overloaded on a node at certain times if large numbers of users concurrently request a service instance to be created. Zhang et al. [30] propose the concept of a Grid mobility service that we feel may be a solution to the serviceoverloading problem. A service could be a mobile code that can move from node to node in a Grid environment. When necessary, a service can move to another more lightly loaded node to spawn service instances. However, practical work needs to be done to serve as proof-of-concept.

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OGSI is a technical implementation speci cation to de ne the interfaces of the core Grid services in the context of OGSA. The GT3 includes an implementation of OGSI. OGSA-DAI is an OGSA compliant middleware technology that can be used speci cally for data access and integration over the Grid. WSRF is emerging as a promising standard for modelling stateful resources with Web services. The work on WSRF is a joint effort put by the Web services and the Grid communities. WSRF will bring the two parties further closer. WSRF is replacing OGSI and will have little impact on OGSA. WSRF can be used as an infrastructure for the construction of the core Grid services in the context of OGSA. WSRF is being taken by the Grid community, e.g. it is expected that WSRF-based GT4 will be released in early 2005.

maximize the organic product going to the organic phase Extraction with solvents heavier than water makes the process operationally easier than the converse, but presents the problem that most such solvents are toxic chlorocarbons Dichloromethane is the least noxious of the bunch Other common extraction solvents are diethyl ether, hydrocarbons, and ethyl acetate With molecules particularly dif cult to extract from the aqueous phase, mixed solvents may prove helpful For example, a mixture of 10 15% isopropanol in a chlorocarbon is one of the most polar organic solutions that is immiscible with water It is quite effective in extracting polar organics such as phosphonates or heterocycles (Fig 101) To ensure easy phase separation when using such solvent mixtures, it is essential to consider densities such that one phase is signi cantly more or less dense than the other.

A qualitative measure of all of the factors contributing to solvent miscibility and therefore utility in phase partitioning (including chromatographic methods) has been developed as the mixotropic solvent series (Appendix 4) The farther two solvents are apart in this series, the less miscible they are The aqueous phase typically is extracted a few times with equal volumes of the organic solvent and the combined organic phases are washed The wash solutions vary with the reaction: NaHCO3 solution and 10% NaOH solution will remove acidic compounds, depending on their pKa, while 5% HCl is used to remove bases NaHSO3 and Na2S2O3 are common reductants used to destroy excess oxidants Saturated CuSO4 solution is very speci c for removing pyridine It forms a blue-purple complex and acts as its own indicator, since the CuSO4 solution is deeply colored when pyridine is present.

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Final washes can be done with brine to remove any traces of water from the organic phase The lessons of solvent extraction from beginning organic chemistry classes should not be forgotten by the aspiring synthetic organic.

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